Crystal Structure Analysis. Principles and Practice (Relié)

Peter Main, William Clegg, Alexander-J Blake, Robert-O Gould

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  • Oxford University Press

  • Paru le : 01/01/2002
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This text focuses on the practical aspects of crystal structure analysis, and provides the necessary conceptual framework for understanding and applying the technique. By choosing an approach that avoids undue emphasis on the mathematics involved, the book gives practical advice on topics such as growing crystals, solving and refining structures, and understanding and using the results. The technique described is a core experimental method in modern structural chemistry, and plays an ever more important role in the careers of graduate students and postdoctoral and academic staff as well as final-year undergraduates. Crystal Structure Analysis has a strong practical orientation. It contains many worked examples and problems (with answers) to reinforce the material presented.
    • A basic introduction to X-ray crystallography
    • Crystal growth, evaluation and mounting
    • Symmetry and space group determination
    • Background theory for data collection
    • Data collection using four-circle diffractometers
    • Area detectors
    • Fourier syntheses
    • Structure determination by Patterson methods
    • Direct methods of crystal structure determination
    • An introduction to maximum entropy
    • Least-squares fitting of parameters
    • Practical aspects of structure refinement
    • The derivation of results
    • The interpretation of results
    • The presentations of results
    • The Crystallographic Information File
    • Crystallographic database
    • Other topics
William Clegg is Professor of Structural Crystallography, University of Newcastle upon Tyne. Alexander J. Blake is Senior Research Officer, School of Chemistry, University of Nottingham. Robert 0. Gould is Honorary Fellow, Institute of Cell and Molecular Biology, University of Edinburgh. Peter Main is Reader in Physics, University of York.

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